Thermal Oxidation Stability of Gear Lubricants

This test is used to determine the deterioration of lubricants, particularly EP gear oils, under severe oxidation conditions. The sample  is  placed in a gear case in which a spur gear  set and a test  bearing  operate under load  while  heat  is applied and  air  is  bubbled  through the oil. The temperature of the  lubricant is  maintained at  325 degree F during  the test. The  above apparatus  and  method were  developed at the  Ordnance Fuels and Lubricants Research  Laboratory, Southwest  Research  Institute, and a report  by Meckel^10  summarizes the  contents as follows: “A description  is given of the  apparatus  recommended  and a list of Purchase Materials, Instructions for Cleaning, Assembling and  Disassembling the  Gearcase. Also  Test Procedure  and  Detail Drawings of the  Assembly are included.”

                                                 

Variations in test  conditions and  their effect  on  oxidation of gear  lubricants, using this spur gear thermal oxidation apparatus, were  reported by Meckel and  Quillian^9 and should  be  consulted  if a  program  of  tests on  the  subject are  to  be made. The test in question is particularly valuable  for  use  in developing  oil additive combinations  which  will  retard  oxidation in  service.

During this test, viscosity of the  oil are  determined at  intervals of  10  hours and  the test  is  concluded  when  the  increase  in  viscosity  reaches  a point  called for in the  specifications.

Specification MIL-L-2105B calls  for a test  time of 50  hours, at  which  time  the  increase  in  viscosity shall  be  a  maximum  of 100 per cent. Also, at the  end  of this  period, the  n-pentane  insolubles must  not  be  more  than  3 per cent  by  weight and  the  benzene insolubles  not  more  than  2 per cent  by weight. Further, the  test  method  requires  inspection of the  various  parts, that  is gears, bearings  and  catalyst,  for the  amount  and  type  of  deposits. The  gear  teeth are  inspected  and any  abnormalities of the  surfaces  noted. After  all  deposits are removed  from the  catalyst, this is  weighed  to  determine  the  copper activity  of the  lubricant. The  test  bearing wear is also  determined  with a  special  fixture and  dial  indicator.

                                                                            

Limitations on Heating of Lubricants for Application

Heavy bodied lubricants, particularly residual types used on exposed gears, are often heated in order to make application easier. If such lubricants are straight mineral oil products, the amount and intensity of heat should not harm them. However, if additives are included, only a very moderate heat should be used. Otherwise some change in the composition is possible. A supplier of the lubricant can advice the limitations on heating. A similar caution is necessary in case lubricating greases are used as gear lubricants. The thickeners for such products may be soaps which upon the application of considerable or prolonged heat will separate from the oil present.