Showing posts with label method. Show all posts
Showing posts with label method. Show all posts

Wednesday, January 2, 2013

Calcium in Lubricating Oil

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While the ASTM Methods and Fed. Test Method use the same sample  for  determination  of  several  metals, the IP  Methods  is  specifically concerned with  calcium  analysis. This calls  for ashing  followed  by determination  of the  calcium  either  as oxide  or oxalate.

Monday, December 31, 2012

Deposit Forming Tendencies of Aircraft Turbine Lubricants

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This test method describes  a procedure for  determining the  deposit  and  sludge  forming  tendencies  of  aircraft gas  turbine  lubricants when  a sample  of the  oil is circulated  under  controlled conditions for a  prescribed  period of time  through an  aerated test  chamber  containing  an  aluminum  tube  held at a constant  temperature.
The coking tube is held at 590 degree F while oil  heated  to  300 degree F  is circulated by  a pump  from  the  chamber through  a  cooler and a line  filter and  back  into  the chamber. The oil flow is regulated to 300 ml per minute while air flow is the same amount.
At  the  end  of the test, the  weight of solid  decomposition  products  on  the  heated tube  and  in the  line after  are  determined. Also,  changes  in the  viscosity and  neutralization  number  of the oil can be  determined  if  desired.




























































































































































































Sulfur in Gear Oils

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In this method  the sample is vaporized  and  burned in a  stream of air, and  the  oxidation completed  by passing  over  quartz particles  maintained  at a temperature  of 950 to 1000 degree C. The combustion  products are then  passed  through hydrogen  peroxide  which  absorbs  the  sulfur  as sulfuric  acid  and  the  chlorine  as hydrochloric  acid. The  absorbent  is then  analyzed  for total  acidity  and  for chloride ion. The  procedure for  the  determination  of  chlorine  is  included  only  for  correcting   the  sulfur  content  and  the  method is not  recommended  for the  determination  of chlorine  alone. 

 

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